Description:

Methods of molecular spectroscopy, fundamental principles. Nuclear magnetic resonance, 1H and 13C NMR techniques in organic structural analysis. Special techniques 2D NMR, COSY, HECTOR. Infrared spectroscopy, fundamental principles. Finger print and practical applications in analysis. UV-VIS spectroscopy, fundamental principles. Mass spectrometry, methods, ionization techniques, fragmentations, applications in structural analysis.

Contents:

.Overview of methods of molecular spectroscopy, fundamental principles.
2.NMR, fundamentals theory and applications.
3.1H NMR in organic structural analysis.
4.13C NMR in organic structural analysis.
5.Special techniques of NMR.
6.2D NMR, COSY and HECTOR.
7.Infrared spectroscopy, fundamental principles and methods.
8.?Finger print? and characteristic vibrations.
9.Practical application of IR in structural analysis.
10.UV-VIS spectroscopy, fundamental principles and methods.
11.Application in structural analysis.
12.Mass spectroscopy, fundamentals, experimental arrangement. 13.Techniques of ionization, pre-separation, basic types of fragmentation.
14.Applications in structural analysis.

Seminar contents:

Interpretation 1H and 13C NMR.
2. Interpretation 2D NMR, COSY and HECTOR.
3. Interpretation IR spectra.
4. Ionization techniques.
5. Interpretation MS.

Recommended literature:

D: Williams D.H., Fleming I.: Spectroscopic methods in organic chemistry. 5. vydání. DH Williams & I Fleming. 9780077091477

Keywords:

IR spectrometry, UV/VIS spectrometry, mass spectrometry

Abbreviations used:

Semester:

• W ... winter semester (usually October - February)
• S ... spring semester (usually March - June)
• W,S ... both semesters

Mode of completion of the course:

• A ... Assessment (no grade is given to this course but credits are awarded. You will receive only P (Passed) of F (Failed) and number of credits)
• GA ... Graded Assessment (a grade is awarded for this course)
• EX ... Examination (a grade is awarded for this course)
• A, EX ... Examination (the award of Assessment is a precondition for taking the Examination in the given subject, a grade is awarded for this course)

Weekly load (hours per week):

• P ... lecture
• C ... seminar
• L ... laboratory
• R ... proseminar
• S ... seminar